Synthesis and Characterization of Nanocrystalline Micro-Mesoporous ZSM-5/MCM-41 Composite Zeolite
Iraqi Journal of Chemical and Petroleum Engineering
View Archive Info| Field | Value | |
| Title |
Synthesis and Characterization of Nanocrystalline Micro-Mesoporous ZSM-5/MCM-41 Composite Zeolite
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| Creator |
Majeed, Najwa Saber
Saleh, Asir Abduljabbar |
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| Description |
Nanocrystalline micro-mesoporous ZSM/MCM-41 composite was synthesized using alkaline treatment method and two step of crystallization in poly tetraflouroethylene (PTFE) lined autoclave. The synthesized zeolites was characterized by X-Ray diffraction (XRD), Scanning electron microscopy (SEM), Transmission electron microscopy (TEM), Atomic force microscopy (AFM), Fourier transport infrared (FTIR), and N2 adsorption-desorption (BET). It was approved that the best results for alkaline leaching can be got with 1.5M NaOH solution. High surface (BET) area of 630 m2/g with pore volume of 0.55 cm3/g has been got. AFM reports showed a nano-level size for average particle size of 50nm.
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| Publisher |
University of Baghdad/ College of Engineering
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| Date |
2016-03-31
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| Type |
info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion |
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| Format |
application/pdf
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| Identifier |
http://ijcpe.uobaghdad.edu.iq/index.php/ijcpe/article/view/91
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| Source |
Iraqi Journal of Chemical and Petroleum Engineering; Vol 17 No 1 (2016): Iraqi Journal of Chemical and Petroleum Engineering; 71-82
المجلة العراقية للهندسة الكيمياوية وهندسة النفط; مجلد 17 عدد 1 (2016): Iraqi Journal of Chemical and Petroleum Engineering; 71-82 2618-0707 1997-4884 |
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| Language |
eng
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| Relation |
http://ijcpe.uobaghdad.edu.iq/index.php/ijcpe/article/view/91/87
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