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Synthesis and Characterization of Iron Oxide Nanoparticles by Open Vessel Ageing Process

Iraqi Journal of Chemical and Petroleum Engineering

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Title Synthesis and Characterization of Iron Oxide Nanoparticles by Open Vessel Ageing Process
 
Creator Majeed, Najwa Saber
Naji, Duaa Mahammed
 
Description Nano-crystalline iron oxide nanoparticles (magnetite) was synthesized by open vessel ageing process. The iron chloride solution was prepared by mixing deionized water and iron chloride tetrahydrate. The product was characterized by X-Ray, Surface area and pore volume by Brunauer-Emmet-Teller, Atomic Force Microscope (AFM) and Fourier Transform Infrared Spectroscopy(FTIR)  .  The results showed that the XRD in compatibility of the prepared iron oxide (magnetite) with the general  structure of standard iron oxide, and in Fourier Transform Infrared Spectroscopy, it is strong crests in 586 bands, because of  the expansion vibration manner related to the metal oxygen absorption band (Fe–O bonds in the crystals of iron oxide). The results show that the prepared nano iron oxide is with average crystal size 75.92 nm,  surface area was 85.97 m2/g and the pore volume  was found equal to 0.1566 cm3/
 
Publisher University of Baghdad/ College of Engineering
 
Date 2018-06-27
 
Type info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
 
Format application/pdf
 
Identifier http://ijcpe.uobaghdad.edu.iq/index.php/ijcpe/article/view/163
 
Source Iraqi Journal of Chemical and Petroleum Engineering; Vol 19 No 2 (2018): Iraqi Journal of Chemical and Petroleum Engineering; 27-31
المجلة العراقية للهندسة الكيمياوية وهندسة النفط; مجلد 19 عدد 2 (2018): Iraqi Journal of Chemical and Petroleum Engineering; 27-31
2618-0707
1997-4884
 
Language eng
 
Relation http://ijcpe.uobaghdad.edu.iq/index.php/ijcpe/article/view/163/159